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N-Formylation of Amines with CO2 and H2 by Using NHC-Iridium Coordination Assemblies as Solid Molecular Catalysts.

Yang ZhangJiaquan WangHaibo ZhuTao Tu
Published in: Chemistry, an Asian journal (2018)
One of the NHC-iridium coordination assemblies containing 1,5-cyclooctadiene (COD) and iodide ion has been demonstrated as robust, efficient, recyclable solid molecular catalyst for N-formylation of diverse primary and secondary amines with CO2 and H2 under mild reaction conditions. Remarkably, in the case of N,N-dimethylformamide production, even at 0.1 mol % catalyst loading under solvent-free conditions, the solid catalyst can be readily recovered by simply filtration and reused more than 10 runs without noticeable loss of activity.
Keyphrases
  • ionic liquid
  • highly efficient
  • room temperature
  • metal organic framework
  • reduced graphene oxide
  • carbon dioxide
  • visible light
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