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Copper-Catalyzed Tandem Cyclization/Direct C(sp 2 )-H Annulation of Azide-Ynamides via α-Imino Copper Carbenes: Access to Azepino[2,3- b :4,5- b ']diindoles.

Yi ChenYao-Hong YanBo-Han ZhuFan ChenLong LiPeng-Cheng Qian
Published in: Organic letters (2023)
A novel copper-catalyzed tandem cyclization/direct C(sp 2 )-H annulation of phenyl azide-ynamides via α-imino copper carbenes has been developed, which provides a concise and flexible approach for the construction of a range of valuable azepino[2,3- b :4,5- b ']diindoles in mostly good to excellent yields with high chemoselectivities. This tandem reaction also exhibits a broad substrate scope, excellent functional group tolerance, simple operation, and mild reaction conditions.
Keyphrases
  • oxide nanoparticles
  • solid state
  • high density