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Two acyclic imides: 3-bromo-N-(3-bromo-benzo-yl)-N-(pyridin-2-yl)benzamide and 3-bromo-N-(3-bromo-benzo-yl)-N-(pyrimidin-2-yl)benzamide.

Féilim DesmondJohn F GallagherNiall Hehir
Published in: Acta crystallographica. Section E, Crystallographic communications (2020)
The title compounds, C19H12Br2N2O2 and C18H11Br2N3O2, were synthesized in good yields from condensation reactions of 3-bromo-benzoyl chloride with 2-amino-pyridine or 2-amino-pyrimidine using standard condensation reaction conditions and subsequent column chromatography.
Keyphrases
  • liquid chromatography
  • high speed
  • tandem mass spectrometry
  • solid phase extraction