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Nano-[Fe 3 O 4 @SiO 2 / N -propyl-1-(thiophen-2-yl)ethanimine][ZnCl 2 ] as a nano magnetite Schiff base complex and heterogeneous catalyst for the synthesis of pyrimido[4,5- b ]quinolones.

Soheila EsmailiAhmad Reza Moosavi-ZareArdeshir Khazaei
Published in: RSC advances (2022)
Nano-[Fe 3 O 4 @SiO 2 / N -propyl-1-(thiophen-2-yl)ethanimine][ZnCl 2 ] as a nano magnetite Schiff base complex was designed and fully characterized by various analyses such as Fourier transform infrared spectroscopy (FT-IR), energy-dispersive X-ray spectroscopy (EDX), X-ray diffraction (XRD), thermal gravimetric analysis (TGA), differential thermal gravimetric analysis (DTA), vibrating sample magnetometry (VSM), scanning electron microscopy (SEM), and transmission electron micrographs (TEM). The presented nano magnetite Schiff base complex was used as a heterogeneous catalyst for the synthesis of pyrimido[4,5- b ]quinolones by the reaction of aryl aldehyde, dimedone and 6-amino-1,3-dimethyluracil in EtOH : H 2 O (7 : 3) as a solvent at 60 °C.
Keyphrases
  • electron microscopy
  • ionic liquid
  • high resolution
  • room temperature
  • highly efficient
  • computed tomography
  • metal organic framework
  • dual energy
  • mass spectrometry
  • contrast enhanced
  • gas chromatography