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Eco Friendly Synthesis of Carbon Dot by Hydrothermal Method for Metal Ions Salt Identification.

Hasan ShabbirTomasz TokarskiDitta UngorMarek Wojnicki
Published in: Materials (Basel, Switzerland) (2021)
In this work, we report the synthesis method of carbon quantum dots (CDs) using the one-step method for fast and effective metal ion determination. Ascorbic acid was used as an inexpensive and environmentally friendly precursor. High-pressure and high-temperature reactors were used for this purpose. Microscopic characterization revealed the size of CDs was in the range of 2-6 nm and they had an ordered structure. The photoluminescence properties of the CDs depend on the process temperature, and we obtained the highest PL spectra for 6 h of hydrothermal reaction. The maximum emission spectra depend poorly on synthesis time. Further characterization shows that CDs are a good contender for sensing Fe 3+ in aqueous systems and can detect concentrations up to 0.49 ppm. The emission spectra efficiency was enhanced by up to 200% with synthesis time.
Keyphrases
  • quantum dots
  • sensitive detection
  • energy transfer
  • high temperature
  • density functional theory
  • photodynamic therapy
  • sewage sludge
  • single cell
  • municipal solid waste