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Crystal structure and Hirshfeld surface analysis of 5-acetyl-3-amino-6-methyl- N -phenyl-4-[( E )-2-phenyl-ethen-yl]thieno[2,3- b ]pyridine-2-carbox-amide.

Shaaban K MohamedEtify A BakhiteSevim Türktekin ÇelikesirHajjaj H M Abdu-AllahMehmet AkkurtOmaima F IbrahimJoel T MagueSafiyyah A H Al-Waleedy
Published in: Acta crystallographica. Section E, Crystallographic communications (2022)
The asymmetric unit of the title compound, C 25 H 21 N 3 O 2 S, comprises four mol-ecules. Their conformations differ primarily in the orientations of the styryl and the N -phenyl-carboxamido groups. In the crystal, inter-molecular N-H⋯N, C-H⋯O and C-H⋯S hydrogen-bonding contacts as well a C-H⋯π(ring) inter-actions lead to the formation of a layer structure parallel to (010). Hirshfeld surface analysis revealed that H⋯H inter-actions represent the main contributions to the crystal packing.
Keyphrases
  • crystal structure
  • solid state