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Synthesis and separation of diastereomeric N-(1-phenylethyl)amides of inherently chiral hydroxydibenzoyloxy-calix[4]arene acetic acids.

Oleksandr O TrybratOleksandr A YesypenkoEduard B RusanovVitali I Kalchenko
Published in: Chirality (2022)
A preparative method for the synthesis of optically pure N-(1-phenylethyl)amides of inherently chiral (cR)- and (cS)-dibenzoyloxy-calix[4]arene acetic acids has been developed. Their absolute stereochemical configuration was determined by X-ray diffraction analysis.
Keyphrases
  • water soluble
  • capillary electrophoresis
  • ionic liquid
  • high resolution
  • electron microscopy
  • magnetic resonance imaging
  • computed tomography
  • mass spectrometry