Low-Cost Benzene Toluene Xylene Measurement Gas System Based on the Mini Chromatographic Cartridge.
Emiliano ZampettiPaolo PapaJoshua AvossaAndrea BearzottiCatia BalducciGiovanna TranfoAntonella MacagnanoPublished in: Sensors (Basel, Switzerland) (2020)
Benzene, toluene and xylene (BTX) are an important part of the volatile organic compounds (VOCs) to be detected and monitored in the air, due to their toxicity towards human health. One of the most reliable technique used in BTX detection is gas chromatography (GC), which presents a high sensitivity. On the other hand, it has important drawbacks, such as high costs, the need for qualified personnel and frequent maintenance. To overcome these drawbacks, this work reports the development of a low cost and portable BTX gas detection system based on a mini chromatographic cartridge, a photo ionization detector (PID), a simple control unit (based on Arduino architecture) and a mini pump. In order to separate the BTX components, we propose the use of a cartridge 80 mm in length, composed of several commercial chromatographic column sections. To test the system performances, we have injected different amounts (from about 0.3 to 5.3 µg) of benzene, toluene and xylene and two of the most frequent possible interferents (ethanol, acetone). Experimental results have shown different retention time values (i.e., 25 ± 0.5 s, 51 ± 1.2 s and 117 ± 4 s, respectively) for benzene, toluene and xylene.
Keyphrases
- low cost
- gas chromatography
- human health
- tandem mass spectrometry
- simultaneous determination
- mass spectrometry
- risk assessment
- liquid chromatography
- solid phase extraction
- high resolution mass spectrometry
- gas chromatography mass spectrometry
- loop mediated isothermal amplification
- label free
- real time pcr
- room temperature
- climate change
- oxidative stress
- emergency department
- magnetic resonance
- carbon dioxide
- adverse drug
- sensitive detection