A Combined Raman Spectroscopy and Atomic Force Microscopy System for In Situ and Real-Time Measures in Electrochemical Cells.
Gianlorenzo BussettiMarco MenegazzoSergei MitkoChiara CastiglioniMatteo TommasiniAndrea LucottiLuca MagagninValeria RussoAndrea Li BassiMartina SienaAlberto GuadagniniSamuele GrilloDavide Del CurtoLamberto DuòPublished in: Materials (Basel, Switzerland) (2023)
An innovative and versatile set-up for in situ and real time measures in an electrochemical cell is described. An original coupling between micro-Raman spectroscopy and atomic force microscopy enables one to collect data on opaque electrodes. This system allows for the correlation of topographic images with chemical maps during the charge exchange occurring in oxidation/reduction processes. The proposed set-up plays a crucial role when reactions, both reversible and non-reversible, are studied step by step during electrochemical reactions and/or when local chemical analysis is required.
Keyphrases
- endoplasmic reticulum stress
- raman spectroscopy
- atomic force microscopy
- induced apoptosis
- high speed
- gold nanoparticles
- single molecule
- ionic liquid
- molecularly imprinted
- label free
- electron transfer
- single cell
- deep learning
- solid state
- electronic health record
- stem cells
- optical coherence tomography
- reduced graphene oxide
- machine learning
- high resolution
- cell therapy
- solid phase extraction
- nitric oxide
- signaling pathway
- cell proliferation