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Two-Photon Absorption and Cell Imaging of Fluorene-Functionalized Epicocconone Analogues.

Samuel OgerDamien SchapmanRomain MougeotStéphane LeleuNoëlle LascouxPatrice BaldeckMagalie BénardThibault GallavardinLudovic GalasXavier Franck
Published in: Chemistry (Weinheim an der Bergstrasse, Germany) (2019)
Epicocconone 1 is a natural chromophore isolated from the fungus Epicoccum nigrum that has shown applications in proteomics and fluorescent microscopy thanks to its unique pro-fluorescence properties. The modification of the skeleton of the natural product by replacing the triene side chain by a fluorenyl scaffold can noticeably increase the fluorophore's absorption coefficient. The synthesis of the analogues of the natural product has been made possible by the use of a palladium-catalyzed carbonylation reaction, allowing the construction of the β-keto-dioxinone key intermediate. Two-photon absorption cross-section measurements of the fluorenyl epicocconone analogues show a structure dependency with values ranging from 60 to 280 GM and live cell imaging show intense staining of intracellular vesicle-like structures around the nucleus.
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