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Silver Decoration of Vertically Aligned MoS 2 -MoO x Nanosheets: A Comprehensive XPS Investigation.

Khaled Al YoussefArkaprava DasJean-François ColomerAxel HembergXavier NoirfaliseCarla Bittencourt
Published in: Materials (Basel, Switzerland) (2024)
This study investigates the simultaneous decoration of vertically aligned molybdenum disulfide nanostructure (VA-MoS 2 ) with Ag nanoparticles (NPs) and nitrogen functionalization. Nitrogen functionalization was achieved through physical vapor deposition (PVD) DC-magnetron sputtering using nitrogen as a reactive gas, aiming to induce p-type behavior in MoS 2 . The utilization of reactive sputtering resulted in the growth of three-dimensional silver structures on the surface of MoS 2 , promoting the formation of silver nanoparticles. A comprehensive characterization was conducted to assess surface modifications and analyze chemical and structural changes. X-ray photoelectron spectroscopy (XPS) showed the presence of silver on the MoS 2 surface. Scanning electron microscopy (SEM) confirmed successful decoration with silver nanoparticles, showing that deposition time affects the size and distribution of the silver on the MoS 2 surface.
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