An ultra-compact low temperature scanning probe microscope for magnetic fields above 30 T.
L RossiJ W GerritsenL NelemansAlexander Ako KhajetooriansB BryantPublished in: The Review of scientific instruments (2018)
We present the design of a highly compact high field scanning probe microscope (HF-SPM) for operation at cryogenic temperatures in an extremely high magnetic field, provided by a water-cooled Bitter magnet able to reach 38 T. The HF-SPM is 14 mm in diameter: an Attocube nano-positioner controls the coarse approach of a piezoresistive atomic force microscopy cantilever to a scanned sample. The Bitter magnet constitutes an extreme environment for scanning probe microscopy (SPM) due to the high level of vibrational noise; the Bitter magnet noise at frequencies up to 300 kHz is characterized, and noise mitigation methods are described. The performance of the HF-SPM is demonstrated by topographic imaging and noise measurements at up to 30 T. Additionally, the use of the SPM as a three-dimensional dilatometer for magnetostriction measurements is demonstrated via measurements on a magnetically frustrated spinel sample.
Keyphrases
- high resolution
- atomic force microscopy
- air pollution
- electron microscopy
- high speed
- living cells
- quantum dots
- single molecule
- climate change
- molecular dynamics simulations
- acute heart failure
- high frequency
- mass spectrometry
- molecular dynamics
- density functional theory
- low cost
- optical coherence tomography
- fluorescent probe
- high throughput
- single cell
- liquid chromatography