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Multimodal x-ray and electron microscopy of the Allende meteorite.

Yuan Hung LoChen-Ting LiaoJihan ZhouArjun RanaCharles S BevisGuan GuiBjoern EndersKevin M CannonYoung-Sang YuRichard S CelestreKasra NowrouziDavid ShapiroHenry Cornelius KapteynRoger W FalconeChristopher J BennettMargaret MurnaneJianwei John Miao
Published in: Science advances (2019)
Multimodal microscopy that combines complementary nanoscale imaging techniques is critical for extracting comprehensive chemical, structural, and functional information, particularly for heterogeneous samples. X-ray microscopy can achieve high-resolution imaging of bulk materials with chemical, magnetic, electronic, and bond orientation contrast, while electron microscopy provides atomic-scale spatial resolution with quantitative elemental composition. Here, we combine x-ray ptychography and scanning transmission x-ray spectromicroscopy with three-dimensional energy-dispersive spectroscopy and electron tomography to perform structural and chemical mapping of an Allende meteorite particle with 15-nm spatial resolution. We use textural and quantitative elemental information to infer the mineral composition and discuss potential processes that occurred before or after accretion. We anticipate that correlative x-ray and electron microscopy overcome the limitations of individual imaging modalities and open up a route to future multiscale nondestructive microscopies of complex functional materials and biological systems.
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