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Halogen Bond Catalyzed Bromocarbocyclization.

Yuk-Cheung ChanYing-Yeung Yeung
Published in: Angewandte Chemie (International ed. in English) (2018)
A halogen bond catalyzed bromo-carbocyclization of N-cinnamyl sulfonamides and O-cinnamyl phenyl ethers has been developed. N-methyl 4-iodopyridinium triflate is used as the halogen-bonding organocatalyst and the reaction is highly chemoselective. This report represents the first proof-of-concept for halogen-bonding organocatalyst-promoted electrophilic halogenation. Mechanistic study suggests the autocatalytic nature of this reaction.
Keyphrases
  • room temperature
  • electron transfer
  • high resolution