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Characterizing Complex Mineral Structures in Thin Sections of Geological Samples with a Scanning Hall Effect Microscope.

Jefferson F D F AraujoAndre L A ReisVanderlei C OliveiraAmanda F SantosCleânio da Luz LimaElder YokoyamaLeonardo A F MendozaJoão M B PereiraAntonio C Bruno
Published in: Sensors (Basel, Switzerland) (2019)
We improved a magnetic scanning microscope for measuring the magnetic properties of minerals in thin sections of geological samples at submillimeter scales. The microscope is comprised of a 200 µm diameter Hall sensor that is located at a distance of 142 µm from the sample; an electromagnet capable of applying up to 500 mT DC magnetic fields to the sample over a 40 mm diameter region; a second Hall sensor arranged in a gradiometric configuration to cancel the background signal applied by the electromagnet and reduce the overall noise in the system; a custom-designed electronics system to bias the sensors and allow adjustments to the background signal cancelation; and a scanning XY stage with micrometer resolution. Our system achieves a spatial resolution of 200 µm with a noise at 6.0 Hz of 300 nTrms/(Hz)1/2 in an unshielded environment. The magnetic moment sensitivity is 1.3 × 10-11 Am². We successfully measured the representative magnetization of a geological sample using an alternative model that takes the sample geometry into account and identified different micrometric characteristics in the sample slice.
Keyphrases
  • high resolution
  • molecularly imprinted
  • electron microscopy
  • computed tomography
  • magnetic resonance
  • optical coherence tomography