Shortening NMR experimental times.
Reika MasudaAbhishek GuptaTimothy Stait-GardnerGang ZhengAllan M TorresWilliam S PricePublished in: Magnetic resonance in chemistry : MRC (2018)
Conventionally, arrayed nuclear magnetic resonance experiments, such as diffusion and relaxation, are performed with the same number of scans (NS) at each iteration despite the signal-to-noise ratio being more than sufficient for many of the iterations. Here, we propose a simple yet effective approach that significantly shortens experimental times by varying NS through the arrayed experiments while keeping the signal-to-noise ratio essentially the same and retaining experimental accuracy.