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Improvement of ultra-small-angle XPCS with the Extremely Brilliant Source.

William ChèvremontThomas ZinnTheyencheri Narayanan
Published in: Journal of synchrotron radiation (2024)
Recent technical developments and the performance of the X-ray photon correlation spectroscopy (XPCS) method over the ultra-small-angle range with the Extremely Brilliant Source (EBS) at the ESRF are described. With higher monochromatic coherent photon flux (∼10 12  photons s -1 ) provided by the EBS and the availability of a fast pixel array detector (EIGER 500K detector operating at 23000 frames s -1 ), XPCS has become more competitive for probing faster dynamics in relatively dilute suspensions. One of the goals of the present development is to increase the user-friendliness of the method. This is achieved by means of a Python-based graphical user interface that enables online visualization and analysis of the processed data. The improved performance of XPCS on the Time-Resolved Ultra-Small-Angle X-ray Scattering instrument (ID02 beamline) is demonstrated using dilute model colloidal suspensions in several different applications.
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