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Status report of the first AMS laboratory in the Czech Republic at the Nuclear Physics Institute, Řež.

Jan KučeraKateřina Pachnerová BrabcováMojmír NěmecJan KameníkJakub TrubačVeronika BrychováIvo SvětlíkJan JohnRoman GarbaMartin Daňo
Published in: Chemicke zvesti (2023)
The first accelerator mass spectrometry (AMS) laboratory in the Czech Republic has been established and put into routine operation in February 2022. Here we briefly describe the facilities available, namely a 300 kV multi-isotope low-energy AMS system (MILEA) capable of determination 10 Be, 14 C, 26 Al, 41 Ca, 129 I, isotopes of U, especially 236 U, Pu and other actinoids, and accessories for 14 C measurements, which include a gas interface system, a preparative gas chromatography system for compound-specific radiocarbon dating analysis, and an isotope-ratio mass spectrometer. The first results achieved for separation and measurement of the above radionuclides (except for 41 Ca) are also reported, with the main focus on 14 C measurements. A specimen breakdown of 729 graphitised samples analysed for 14 C so far is presented, as well as a proof of measurement stability of the MILEA system obtained by analysis of radiocarbon standards and analytical blanks. For the other radionuclides, well proven or novel procedures for sample preparation and measurement are presented.
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