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Amorphous FeNiCu-MOFs as highly efficient electrocatalysts for the oxygen evolution reaction in an alkaline medium.

Hao WuQingxi ZhaiFan DingDongyue SunYujie MaYilun RenBiao WangFengqi LiHaifeng BianYurong YangLan ChenShaochun TangXiangkang Meng
Published in: Dalton transactions (Cambridge, England : 2003) (2022)
The preparation of low-cost and high-activity oxygen evolution reaction (OER) catalysts is a technical bottleneck in the field of electrolysis of water to produce hydrogen. Amorphous metal-organic frameworks (MOFs) with low-cost transition metals have attracted increasing attention in the catalytic field, yet metal atoms that are the main active sites are still ambiguous. Here, we synthesized a series of amorphous ternary Fe x (NiCu) 3- x -MOFs via an ultrasonic method. The optimal amorphous FeNiCu-MOF is found to be able to supply a current density of 10 mA cm -2 merely at a low overpotential of 260 mV with a small Tafel slope of 61 mV dec -1 and exhibits high durability over 24 h. Moreover, density functional theory (DFT) calculations show that the Fe atoms are the main active sites for the OER in the FeNiCu-MOF. This work shows that amorphous ternary MOFs have great potential for application in OER electrocatalysts due to the multiple synergistic effects and amorphous MOF structures.
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