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Metal-Free Radical [2 + 2 + 1] Cyclization of ortho-Cyanoarylacrylamides with Alkyl Nitriles: Synthesis of Pyrrolo[3,2- c]quinolines.

Tao YangWen-Jin XiaJia-Qi ShangYi LiXiang-Xiang WangMeng SunYa-Min Li
Published in: Organic letters (2018)
A novel radical [2 + 2 + 1] cyclization of ortho-cyanoarylacrylamides with dual α-C-H bonds in alkyl nitriles has been developed. The reaction provides new facile and straightforward access to cyano-substituted pyrrolo[3,2- c]quinolines, which are important nitrogen-containing polyheterocycles. A possible mechanism for the transformation is proposed.
Keyphrases
  • ionic liquid
  • visible light
  • molecular docking
  • quantum dots
  • reduced graphene oxide
  • metal organic framework
  • molecular dynamics simulations