Rapid and simple identification of trace amounts of sodium azide in beverages and bodily fluids followed by derivatization and liquid chromatography-electrospray ionization tandem mass spectrometry.
Hagit PrihedAvital ShifrovitchTamar Shamai YaminMoran MadmonChen BelayMerav BlancaAvi WeissbergPublished in: Rapid communications in mass spectrometry : RCM (2023)
Compared with previously reported chromatography-based methods, this method that was based on derivatization and LC/ESI-MS/MS analysis was substantially more sensitive, simpler and faster. The method can be used for forensic investigation to confirm azide exposure from fatal use to much smaller intoxication dose.
Keyphrases
- tandem mass spectrometry
- liquid chromatography
- ultra high performance liquid chromatography
- ms ms
- high performance liquid chromatography
- simultaneous determination
- mass spectrometry
- gas chromatography
- high resolution mass spectrometry
- liquid chromatography tandem mass spectrometry
- solid phase extraction
- high resolution
- gas chromatography mass spectrometry
- heavy metals