Determination of Multi-pesticides Residues in Jasmine Flower and Its Scented Tea.
Yilu ZhouYangliu WuWenbo ZengQuanshun AnGuanyu ChenCanping PanPublished in: Bulletin of environmental contamination and toxicology (2023)
For minor crops such as jasmine, the lack of pesticide registration and maximum residue limits are important issues that need to be solved in order to facilitate trading and ensure food safety. Meanwhile, reliable and quick analytical methods for multi-pesticide residues in these commodities are few, but required by various stakeholders. In this study, a method for detecting twenty-five most frequently used pesticides in jasmine flower and its scented tea by multi-plug filtration cleanup and ultra-high-performance liquid chromatography-tandem mass spectrometry was developed and validated. The cleanup process was optimized and compared with the dispersive solid phase extraction procedure. The method was validated, showing that except for methomyl, recoveries of twenty-five pesticides were 64%-108%, with relative standard deviations (n = 5) of 0.33%-10%. The method was successfully applied to detect pesticide residues in marketed samples. The results showed that some flower and tea samples contained a combination of different pesticide residues.
Keyphrases
- solid phase extraction
- risk assessment
- liquid chromatography tandem mass spectrometry
- gas chromatography
- molecularly imprinted
- high performance liquid chromatography
- liquid chromatography
- tandem mass spectrometry
- simultaneous determination
- human health
- gas chromatography mass spectrometry
- ultra high performance liquid chromatography
- mass spectrometry
- high resolution mass spectrometry
- high resolution
- minimally invasive
- ms ms
- ionic liquid