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Enhancement of peroxymonosulfate activation with nickel foam-supported CuCo 2 O 4 for tetracycline degradation: Performance and mechanism insights.

Hairui LiChang LiuZhonghua MouPeng YuShiqi WuWei WangZhaohui WangRuixia Yuan
Published in: Journal of colloid and interface science (2024)
The modulation of bimetallic oxide structures and development of efficient, easily recoverable catalysts are expected to effectively overcome the limitations associated with powdered catalysts in activating peroxymonosulfate (PMS). In this study, CuCo 2 O 4 was successfully immobilized on the surface of nickel foam (NF) via an electrodeposition-calcination procedure, with highly efficient activation of PMS for tetracycline (TC) degradation (0.55 min -1 ). Besides acting as a support carrier and providing ample active sites, NF mediated electron transport, prevented the leaching of metal ions and enhanced the efficiency of recycling. Density functional theory (DFT) calculations and experimental tests illustrated that Cu/Co dual-sites can efficiently adsorb PMS, enabling simultaneous reduction and oxidation reactions. The dual-site synergy substantially decreased the adsorption barrier and increased the electron transfer rate. Especially, the Cu + /Cu 2+ redox couple acted as an electron donor and facilitated rapid charge transfer, leading to the conversion of Co 3+ to Co 2+ . Moreover, the CuCo 2 O 4 @NF + PMS system effectively eliminated TC by employing radical pathways (SO 4 •- , • OH) and nonradical processes ( 1 O 2 , e - ). Therefore, this study introduces a new approach to overcome the limitations of powdered bimetallic oxides, providing a promising solution for practical applications.
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