Pentafluorobenzylation and detection of sodium monofluoroacetate (compound 1080) in veterinary samples using gas chromatography/tandem quadrupole mass spectrometry with multiple reaction monitoring.
John P BuchweitzMargaret JohnsonAndreas F LehnerPublished in: Rapid communications in mass spectrometry : RCM (2021)
The method was validated with a calculated limit of detection of 0.35 ppm and limit of quantitation of 1.09 ppm MFA. The method should have adequate sensitivity and reliability for veterinary toxicology labs analyzing specimens from animals poisoned by this predacide.
Keyphrases
- mass spectrometry
- gas chromatography
- tandem mass spectrometry
- liquid chromatography
- high performance liquid chromatography
- high resolution mass spectrometry
- capillary electrophoresis
- solid phase extraction
- loop mediated isothermal amplification
- gas chromatography mass spectrometry
- high resolution
- label free
- real time pcr
- ms ms
- simultaneous determination
- electron transfer