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Direct Amination of α-Hydroxy Amides.

Ajay L ChandgudeAlexander Dömling
Published in: Asian journal of organic chemistry (2017)
A TiCl4-mediated reaction for the direct amination of α-hydroxy amides has been developed. This simple, general, additive/base/ligand-free reaction is mediated by economical TiCl4. The reaction runs under mild conditions. This highly efficient C-N bond formation protocol is valid for diverse amines, including primary, secondary and heterocyclic amines, and even a primary amide and indole.
Keyphrases
  • highly efficient
  • randomized controlled trial
  • electron transfer
  • visible light